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MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight
Tooley, O. Pointer, W. Radmall, R. Hall, M. Beyer, V. Stakem, K. Town, J. Junkers, T. Wilson, P.
Tooley, O.
Pointer, W.
Radmall, R.
Hall, M.
Beyer, V.
Stakem, K.
Town, J.
Junkers, T.
Wilson, P.
Publication Date
2024
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© 2024 The Authors. Macromolecular Rapid Communications published by Wiley-VCH GmbH
This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
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2024-01
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Abstract
Measurement of molecular weight is an integral part of macromolecular and polymer characterization which usually has limitations. Herein, we present the use of a bench-top 80 MHz NMR spectrometer for diffusion-ordered spectroscopy as a practical and rapid approach for the determination of molecular weight/size using a novel solvent and polymer-independent universal calibration.
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Citation
Tooley O, Pointer W, Radmall R et al (2024) MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight. Macromolecular Rapid Communications. Accepted for Publication.
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Article