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    Stabilisation of metastable polymorphs: the case of paracetamol form III

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    Publication date
    2016
    Author
    Telford, Richard
    Seaton, Colin C.
    Clout, A.
    Buanz, A.B.M.
    Gaisford, S.
    Williams, G.R.
    Prior, T.J.
    Okoye, C.H.
    Munshi, Tasnim
    Scowen, Ian J.
    Keyword
    Metastable polymorphs; Paracetamol form III; Air-stable formulation; Melt synthesis; Melt crystallisation
    Rights
    (c) 2016 The Authors. This is an Open Access article licensed under the Creative Commons CC-BY license (http://creativecommons.org/licenses/by-nc/3.0/)
    Peer-Reviewed
    Yes
    
    Metadata
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    Abstract
    The design of a melt synthesis of the first air-stable formulation of the metastable form III of paracetamol is derived from thermo-spectroscopic and thermo-diffraction experiments. Melt crystallisation in the presence of β-1,4-saccharides produces form III selectively and the excipients appear to act as stabilising ‘active’ templates of the metastable polymorph.
    URI
    http://hdl.handle.net/10454/8921
    Version
    published version paper
    Citation
    Telford R, Seaton CC, Clout A et al (2016) Stabilisation of metastable polymorphs: the case of paracetamol form III. Chemical Communications. Accepted for publication.
    Link to publisher’s version
    http://dx.doi.org/10.1039/C6CC05006A
    Type
    Article
    Notes
    This article is part of themed collection: Pharmaceutical Solids.
    Collections
    Life Sciences Publications

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