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    A safe, convenient and efficient method for the preparation of heterocyclic N-oxides using urea-hydrogen peroxide

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    Publication date
    2008
    Author
    Rong, Dawen
    Phillips, Victoria A.
    Rubio, R.S.
    Angeles Castro, M.
    Wheelhouse, Richard T.
    Keyword
    REF 2014; N-Oxide; Urea·hydrogen peroxide; Trifluoroperacetic acid; Pyrimidine; Pyridine; Quinoline
    
    Metadata
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    Abstract
    A novel, convenient, and high-yielding method has been developed for the preparation of heterocyclic N-oxides. The reaction uses the urea·hydrogen peroxide addition complex as a peroxide source for the in situ generation of trifluoroperacetic acid. The advantages of this method are easy handling of a stable, solid oxidant; high yields and simple removal of excess reagents and by-products.
    URI
    http://hdl.handle.net/10454/6160
    Citation
    Rong, D., Phillips, Victoria A., Rubio, Ramon Sanchez, Angeles Castro, Ma, Wheelhouse, Richard T. (2008) A safe, convenient and efficient method for the preparation of heterocyclic N-oxides using urea-hydrogen peroxide. Tetrahedron Letters, 49 (48), 6933-6935.
    Link to publisher’s version
    http://dx.doi.org/10.1016/j.tetlet.2008.09.124
    Type
    Article
    Collections
    Life Sciences Publications

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