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    Crystal Structure of a Rigid Ferrocence-based Macrocycle from High-Resolution X-ray Powder Diffraction.

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    Publication date
    2001
    Author
    Dinnebier, R.E.
    Ding, L.
    Ma, K.
    Neumann, M.A.
    Tanpipat, N.
    Leusen, Frank J.J.
    Stephens, P.W.
    Wagner, M.
    Keyword
    Crystal Structure
    High-Resolution X-ray Powder Diffraction
    Organometallics
    Peer-Reviewed
    Yes
    
    Metadata
    Show full item record
    Abstract
    A macrocycle, 6, has been synthesized in high yield from 2,5-di(pyrazol-1-yl)hydroquinone and 1,1`-fc[B(Me)NMe2]2 {fc = Fe(C5H4)2}. The molecule incorporates two redox-active 1,1`-ferrocenylene units in its backbone and contains four chiral boron centers, each of them possessing the same configuration. It is demonstrated that crystal structures of organometallics of moderate complexity can be solved from high-resolution X-ray powder diffraction patterns, once the connectivity between the functional groups is known.
    URI
    http://hdl.handle.net/10454/3984
    Version
    No full-text available in the repository
    Citation
    Dinnebier, R.E., Ding, L., Ma, K. and Leusen, F.J.J. (2001). Crystal Structure of a Rigid Ferrocence-based Macrocycle from High-Resolution X-ray Powder Diffraction. Organometallics. Vol. 20, No. 26, pp. 5642-5647.
    Link to publisher’s version
    http://pubs.acs.org/doi/full/10.1021/om0105066
    Type
    Article
    Collections
    Life Sciences Publications

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