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Synthesis and structural studies (H-1, C-13, P-31 NMR and X-ray) of new C-bonded cyclotriphosphazenes with heterocyclic substituents from novel phosphinic acid derivatives.

dc.contributor.authorVicente, V.*
dc.contributor.authorFruchier, A.*
dc.contributor.authorTaillefer, M.*
dc.contributor.authorCoombes-Chamelet, C.*
dc.contributor.authorScowen, Ian J.*
dc.contributor.authorPlenat, F.*
dc.contributor.authorCristeau, H-J.*
dc.date.accessioned2009-09-30T09:25:55Z
dc.date.available2009-09-30T09:25:55Z
dc.date.issued2004
dc.identifier.citationVicente, V., Fruchier, A., Taillefer, M., Coombes-Chamelet, C. and Scowen, I.J. et al. (2004). Synthesis and structural studies (H-1, C-13, P-31 NMR and X-ray) of new C-bonded cyclotriphosphazenes with heterocyclic substituents from novel phosphinic acid derivatives. New Journal of Chemistry. Vol. 28, No. 3, pp. 418-424.
dc.identifier.urihttp://hdl.handle.net/10454/3552
dc.descriptionNo
dc.description.abstractThree new C-bonded cyclotriphosphazenes, [N3P3(2-thienyl)6], 2, [N3P3(3-thienyl)6], 4, and [N3P3(3,3-bithienyl-2,2-ylene)3], 6, have been prepared by two new synthetic procedures and are the first examples of non-spiro and trispirocyclotriphosphazene derivatives composed of thiophene and 3,3-dithiophene substituents, respectively. Their 1H, 13C and 31P NMR parameters are given. The solid state structures of 2, 4 and 6 have been determined by X-ray crystallography.
dc.language.isoen
dc.subjectCoupling-constants
dc.subjectPhosphorus-nitrogen compounds
dc.subjectCrystal-structure
dc.subjectSpectra nuclei
dc.titleSynthesis and structural studies (H-1, C-13, P-31 NMR and X-ray) of new C-bonded cyclotriphosphazenes with heterocyclic substituents from novel phosphinic acid derivatives.
dc.status.refereedYes
dc.typeArticle
dc.type.versionNo full-text in the repository
dc.identifier.doihttps://doi.org/10.1039/b311046j
dc.openaccess.statusclosedAccess


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