MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight

Tooley, O.; Pointer, W.; Radmall, R.; Hall, M.; Beyer, V.; Stakem, K.; Swift, Thomas; Town, J.; Junkers, T.; Wilson, P.; Lester, D.; Hadleton, D.

dc.contributor.author	Tooley, O.
dc.contributor.author	Pointer, W.
dc.contributor.author	Radmall, R.
dc.contributor.author	Hall, M.
dc.contributor.author	Beyer, V.
dc.contributor.author	Stakem, K.
dc.contributor.author	Swift, Thomas
dc.contributor.author	Town, J.
dc.contributor.author	Junkers, T.
dc.contributor.author	Wilson, P.
dc.contributor.author	Lester, D.
dc.contributor.author	Hadleton, D.
dc.date.accessioned	2024-03-03T20:15:41Z
dc.date.accessioned	2024-04-03T11:54:00Z
dc.date.available	2024-03-03T20:15:41Z
dc.date.available	2024-04-03T11:54:00Z
dc.date.issued	2024
dc.identifier.citation	Tooley O, Pointer W, Radmall R et al (2024) MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight. Macromolecular Rapid Communications. Accepted for Publication.
dc.identifier.uri	http://hdl.handle.net/10454/19863
dc.description	Yes
dc.description.abstract	Measurement of molecular weight is an integral part of macromolecular and polymer characterization which usually has limitations. Herein, we present the use of a bench-top 80 MHz NMR spectrometer for diffusion-ordered spectroscopy as a practical and rapid approach for the determination of molecular weight/size using a novel solvent and polymer-independent universal calibration.
dc.description.sponsorship	Royal Society. Grant Number: URF∖R1∖180274. Engineering and Physical Sciences Research Council. Grant Numbers: EP/V037943/1, EP/V007688/1, EP/V036211/1
dc.language.iso	en
dc.rights	© 2024 The Authors. Macromolecular Rapid Communications published by Wiley-VCH GmbH This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
dc.subject	Diffusion-ordered spectroscopy
dc.subject	Macromolecule
dc.subject	Molecular weight
dc.subject	NMR spectroscopy
dc.subject	Polymer
dc.title	MaDDOSY (Mass Determination Diffusion Ordered Spectroscopy) using an 80 MHz bench top NMR for the rapid determination of polymer and macromolecular molecular weight
dc.status.refereed	Yes
dc.date.application	2024-01-30
dc.type	Article
dc.type.version	Published version
dc.identifier.doi	https://doi.org/10.1002/marc.202300692
dc.rights.license	CC-BY
dc.date.updated	2024-03-03T20:15:43Z
refterms.dateFOA	2024-04-03T11:54:30Z
dc.openaccess.status	openAccess
dc.date.accepted	2024-01