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    Interfacial cocrystallization using oily phase via liquid−liquid phase separation

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    Sajid_et_al_Crystal_Growth_&_Design.pdf (4.497Mb)
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    Publication date
    2022-10
    Author
    Sajid, Asim
    Alsirawan, M.H.D. Bashir
    Seaton, Colin C.
    Swift, Thomas
    Pagire, Sudhir K.
    Vangala, Venu R.
    Kelly, Adrian L.
    Paradkar, Anant R.
    Keyword
    Crystallization
    Crystals
    Kinetic modeling
    Solution chemistry
    Solvents
    Oily phase liquid–liquid phase separation (LLPS)
    Research Development Fund Publication Prize Award
    Rights
    © 2022 The Authors. Published by American Chemical Society. This work is licensed under a Creative Commons Attribution 4.0 International License. http://creativecommons.org/licenses/by/4.0/
    Peer-Reviewed
    Yes
    Open Access status
    openAccess
    
    Metadata
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    Abstract
    Cocrystals consist of two molecules bonded together in a single crystal lattice giving rise to wide applications including improving solubility of poorly soluble pharmaceuticals. Cocrystallization reaction occurs in the oily phase of liquid–liquid phase separation (LLPS) after it is mixed with coformers. Indomethacin–saccharin cocrystal formation was monitored in situ, and the kinetics of crystallization were determined. The crystallization rates show that the process can be proposed to prevent unwanted oily phase formation during LLPS.
    URI
    http://hdl.handle.net/10454/19177
    Version
    Published version
    Citation
    Al-Hanafi Sajid A, Alsirawan MHDB, Seaton CC et al (2022) Interfacial cocrystallization using oily phase via liquid−liquid phase separation. Crystal, Growth & Design. 22(10): 5845-5851.
    Link to publisher’s version
    https://doi.org/10.1021/acs.cgd.2c00263
    Type
    Article
    Notes
    Research Development Fund Publication Prize Award winner, Sep 2022.
    Collections
    Life Sciences Publications

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