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    Recent developments in mechanochemical materials synthesis by extrusion

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    Publication date
    2016-07
    Author
    Crawford, Deborah E.
    Casaban, J.
    Keyword
    Mechanochemistry
    Extrusion
    Scale-up
    MOFs
    Synthesis
    Peer-Reviewed
    Yes
    
    Metadata
    Show full item record
    Abstract
    Mechanochemical synthesis, i.e., reactions conducted by grinding solid reactants together with no or minimal solvent, has been demonstrated as an excellent technique for the formation of both organic and inorganic compounds. Mechanochemistry is viewed as an alternative approach to chemical synthesis and is not always considered when developing manufacturing processes of fine chemicals. Here, recent advances are highlighted regarding mechanochemical synthesis, by utilizing a well‐developed continuous technique – extrusion, and the advantages it offers to further support its use in the manufacturing of these chemicals. To put this work into context, it is shown how extrusion plays a vital role for manufacturing in the food, polymer, and pharmaceutical industries, and how the research carried out by these respective industrialists provides great insight and understanding of the technique, with the results being applicable in the chemical industry. The synthesis of metal–organic frameworks (MOFs) is highlighted herein as an excellent example showcasing the advantages that extrusion provides to the manufacture of these materials, one advantage being the exceptional space time yields (STYs) reported for these processes, at three orders of magnitude greater than conventional (solvothermal) synthesis.
    URI
    http://hdl.handle.net/10454/17694
    Version
    No full-text in the repository
    Citation
    Crawford DE and Casaban J (2016) Recent developments in mechanochemical materials synthesis by extrusion. Advanced Materials. 28(27): 5747-5754.
    Link to publisher’s version
    https://doi.org/10.1002/adma.201505352
    Type
    Article
    Collections
    Life Sciences Publications

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