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    Extrusion - back to the future: using an established technique to reform automated chemical synthesis

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    Crawford_Beilstein_Jnl_of_Organic_Chemistry.pdf (2.152Mb)
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    Publication date
    2017-01
    Author
    Crawford, Deborah E.
    Keyword
    Continuous
    Extrusion
    Industry
    Organic
    Synthesis
    Rights
    © 2017 Crawford; licensee Beilstein-Institut. This is an Open Access article under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
    Peer-Reviewed
    Yes
    
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    Abstract
    Herein, the benefits which extrusion can provide for the automated continuous synthesis of organic compounds are highlighted. Extrusion is a well-established technique that has a vital role in the manufacturing processes of polymers, pharmaceuticals and food products. Furthermore, this technique has recently been applied to the solvent-free continuous synthesis of co-crystals and coordination compounds including metal-organic frameworks (MOFs). To date, a vast amount of research has already been conducted into reactive extrusion (REX), particularly in the polymer industry, which in many cases has involved organic transformations, however, it has not received significant recognition for this. This review highlights these transformations and discusses how this previous research can be applied to the future of organic compound manufacture.
    URI
    http://hdl.handle.net/10454/17689
    Version
    Published version
    Citation
    Crawford DE (2017) Extrusion - back to the future: using an established technique to reform automated chemical synthesis. Beilstein Journal of Organic Chemistry. 13: 65-75.
    Link to publisher’s version
    https://doi.org/10.3762/bjoc.13.9
    Type
    Article
    Collections
    Life Sciences Publications

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