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    Polynuclear complexes as precursor templates for hierarchical microporous graphitic carbon: An unusual approach

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    Nayak_et_al_ACS_AMI_Final.pdf (6.984Mb)
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    Publication date
    2018-07
    Author
    Kobielska, P.A.
    Telford, Richard
    Rowlandson, J.
    Tian, M.
    Shahin, Z.
    Demessence, A.
    Ting, V.P.
    Nayak, Sanjit
    Keyword
    Complex-derived carbon
    Coordination complex
    Graphitic carbon
    Hydrogen storage
    Polynuclear complex
    Porous carbon
    Template precursor
    Rights
    This document is the Accepted Manuscript version of a Published Work that appeared in final form in ACS Applied Materials & Interfaces, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://dx.doi.org/10.1021/acsami.8b10149
    Peer-Reviewed
    Yes
    
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    Abstract
    A highly porous carbon was synthesized using a coordination complex as an unusual precursor. During controlled pyrolysis, a trinuclear copper complex, [CuII3Cl4(H2L)2]·CH3OH, undergoes phase changes with melt and expulsion of different gases to produce a unique morphology of copper-doped carbon which, upon acid treatment, produces highly porous graphitic carbon with a surface area of 857 m2 g–1 and a gravimetric hydrogen uptake of 1.1 wt % at 0.5 bar pressure at 77 K.
    URI
    http://hdl.handle.net/10454/16535
    Version
    Accepted Manuscript
    Citation
    Kobielska PA, Telford R, Rowlandson J et al (2018) Polynuclear complexes as precursor templates for hierarchical microporous graphitic carbon: An unusual approach. ACS Applied Materials & Interfaces. 10(31): 25967-25971.
    Link to publisher’s version
    http://dx.doi.org/10.1021/acsami.8b10149
    Type
    Article
    Collections
    Life Sciences Publications

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