BRADFORD SCHOLARS

    • Sign in
    View Item 
    •   Bradford Scholars
    • Engineering and Informatics
    • Engineering and Informatics Publications
    • View Item
    •   Bradford Scholars
    • Engineering and Informatics
    • Engineering and Informatics Publications
    • View Item
    JavaScript is disabled for your browser. Some features of this site may not work without it.

    Browse

    All of Bradford ScholarsCommunitiesAuthorsTitlesSubjectsPublication DateThis CollectionAuthorsTitlesSubjectsPublication Date

    My Account

    Sign in

    HELP

    Bradford Scholars FAQsCopyright Fact SheetPolicies Fact SheetDeposit Terms and ConditionsDigital Preservation Policy

    Statistics

    Most Popular ItemsStatistics by CountryMost Popular Authors

    Feasibility of novel integrated dividing-wall batch reactive distillation processes for the synthesis of methyl decanoate

    • CSV
    • RefMan
    • EndNote
    • BibTex
    • RefWorks
    Thumbnail
    View/Open
    Mujtaba_et_al_Separation_and_Purification_Technology.pdf (796.8Kb)
    Download
    Publication date
    2018-08-31
    Author
    Aqar, D.Y.
    Rahmanian, Nejat
    Mujtaba, Iqbal M.
    Keyword
    Dynamic modelling; Optimization; Energy usage; Methyl decanoate; i-DWBD; Esterification
    Rights
    © 2018 Elsevier B.V. Reproduced in accordance with the publisher's self-archiving policy. This manuscript version is made available under the CC-BY-NC-ND 4.0 license.
    Peer-Reviewed
    Yes
    
    Metadata
    Show full item record
    Abstract
    The production of methyl decanoate (MeDC) through esterification of decanoic acid (DeC) with methanol by reactive distillation is operationally challenging and energy-intensive due to the complicated behaviour of the reaction system and the difficulty of retaining the reactants together in the reaction region. Methanol being the lightest component in the mixture can separate itself from the reactant DeC as the distillation proceeds which will cause a massive reduction in the conversion of DeC utilizing either a batch or continuous distillation process. Aiming to overcome this type of the potential problem, novel integrated divided-wall batch reactive distillation configuration (i-DWBD) with recycling from the distillate tank is established in this study and is examined in detail. This study has clearly demonstrated that the integrated divided-wall batch reactive distillation column (i-DWBD) is superior to the traditional conventional batch distillation (CBD) and both the divided-wall (DWBD), and split reflux divided-wall (sr-DWBD) batch reactive distillation configurations in terms of maximum achievable purity of MeDC and higher conversion of DeC into MeDC. In addition, significant batch time and energy savings are possible when the i-DWBD is operated in multi-reflux mode.
    URI
    http://hdl.handle.net/10454/15361
    Version
    Accepted Manuscript
    Citation
    Aqar DY, Rahmanian N and Mujtaba IM (2018) Feasibility of novel integrated dividing-wall batch reactive distillation processes for the synthesis of methyl decanoate. Separation and Purification Technology. 202: 200-215.
    Link to publisher’s version
    https://doi.org/10.1016/j.seppur.2018.03.025
    Type
    Article
    Collections
    Engineering and Informatics Publications

    entitlement

     
    DSpace software (copyright © 2002 - 2023)  DuraSpace
    Quick Guide | Contact Us
    Open Repository is a service operated by 
    Atmire NV
     

    Export search results

    The export option will allow you to export the current search results of the entered query to a file. Different formats are available for download. To export the items, click on the button corresponding with the preferred download format.

    By default, clicking on the export buttons will result in a download of the allowed maximum amount of items.

    To select a subset of the search results, click "Selective Export" button and make a selection of the items you want to export. The amount of items that can be exported at once is similarly restricted as the full export.

    After making a selection, click one of the export format buttons. The amount of items that will be exported is indicated in the bubble next to export format.