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dc.contributor.authorPitto-Barry, Anaïs*
dc.contributor.authorPerdigao, L.M.A.*
dc.contributor.authorWalker, M.*
dc.contributor.authorLawrence, J.*
dc.contributor.authorConstantini, G.*
dc.contributor.authorSadler, P.J.*
dc.contributor.authorBarry, Nicolas P.E.*
dc.date.accessioned2017-02-01T15:30:24Z
dc.date.available2017-02-01T15:30:24Z
dc.date.issued2015
dc.identifier.citationPitto-Barry A, Perdigao LMA, Walker M et al (2015) Synthesis and controlled growth of osmium nanoparticles by electron irradiation. Dalton Transactions. 44(47): 20308-20311.en_US
dc.identifier.urihttp://hdl.handle.net/10454/11237
dc.descriptionYesen_US
dc.description.abstractWe have synthesised osmium nanoparticles of defined size (1.5–50 nm) on a B- and S-doped turbostratic graphitic structure by electron-beam irradiation of an organometallic osmium complex encapsulated in self-spreading polymer micelles, and characterised them by transmission electron microscopy (TEM), high-resolution TEM (HRTEM), and atomic force microscopy (AFM) on the same grid. Oxidation of the osmium nanoparticles after exposure to air was detected by X-ray photoelectron spectroscopy (XPS).en_US
dc.description.sponsorshipWe thank the Leverhulme Trust (Early Career Fellowship No. ECF-2013-414 to NPEB), the University of Warwick (Grant No. RD14102 to NPEB), the ERC (Grant No. 247450 to PJS), and the EPSRC (EP/F034210/1 to PJS). L.M.A.P., J.L., and G.C. acknowledge financial support from the EU through the ERC Consolidator Grant “VISUAL-MS”.en_US
dc.language.isoenen_US
dc.relation.isreferencedbyhttp://dx.doi.org/10.1039/C5DT03205Aen_US
dc.rights© 2015 The Royal Society of Chemistry. Reproduced in accordance with the publisher's self-archiving policy. This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.en_US
dc.subjectOsmium nanoparticles; Synthesis and controlled growth; Electron-beam irradiationen_US
dc.titleSynthesis and controlled growth of osmium nanoparticles by electron irradiationen_US
dc.status.refereedYesen_US
dc.date.Accepted2015-09-14
dc.date.application2015-09-29
dc.typeArticleen_US
dc.type.versionPublished versionen_US
refterms.dateFOA2018-07-26T09:44:46Z


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