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    Synthesis and controlled growth of osmium nanoparticles by electron irradiation

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    Barry_Dalton_Transactions_2015.pdf (1.306Mb)
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    Publication date
    2015
    Author
    Pitto-Barry, Anaïs
    Perdigao, L.M.A.
    Walker, M.
    Lawrence, J.
    Constantini, G.
    Sadler, P.J.
    Barry, Nicolas P.E.
    Keyword
    Osmium nanoparticles; Synthesis and controlled growth; Electron-beam irradiation
    Rights
    © 2015 The Royal Society of Chemistry. Reproduced in accordance with the publisher's self-archiving policy. This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
    Peer-Reviewed
    Yes
    
    Metadata
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    Abstract
    We have synthesised osmium nanoparticles of defined size (1.5–50 nm) on a B- and S-doped turbostratic graphitic structure by electron-beam irradiation of an organometallic osmium complex encapsulated in self-spreading polymer micelles, and characterised them by transmission electron microscopy (TEM), high-resolution TEM (HRTEM), and atomic force microscopy (AFM) on the same grid. Oxidation of the osmium nanoparticles after exposure to air was detected by X-ray photoelectron spectroscopy (XPS).
    URI
    http://hdl.handle.net/10454/11237
    Version
    Published version
    Citation
    Pitto-Barry A, Perdigao LMA, Walker M et al (2015) Synthesis and controlled growth of osmium nanoparticles by electron irradiation. Dalton Transactions. 44(47): 20308-20311.
    Link to publisher’s version
    http://dx.doi.org/10.1039/C5DT03205A
    Type
    Article
    Collections
    Life Sciences Publications

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