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    A multinuclear 1H, 13C and 11B solid-state MAS NMR study of 16- and 18-electron organometallic ruthenium and osmium carborane complexes

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    Publication date
    2014-02
    Author
    Barry, Nicolas P.E.
    Kemp, T.F.
    Sadler, P.J.
    Hanna, J.V.
    Keyword
    Carboranes; ruthenium and osmium complexes; MAS NMR data
    Rights
    © 2014 The Royal Society of Chemistry. Reproduced in accordance with the publisher's self-archiving policy. This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
    Peer-Reviewed
    Yes
    
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    Abstract
    The first 1H, 13C, 31P and 11B solid state MAS NMR studies of electron- deficient carborane-containing ruthenium and osmium complexes [Ru/Os(p-cym)(1,2-dicarba-closo-dodecaborane-1,2- dithiolate)] are reported. The MAS NMR data from these 16-electron complexes are compared to those of free carborane-ligand and an 18-electron triphenylphosphine ruthenium adduct, and reveal clear spectral differences between 16- and 18-electron organometallic carborane systems in the solid state.
    URI
    http://hdl.handle.net/10454/11200
    Version
    Published version
    Citation
    Barry NPE, Kemp TF, Sadler PJ et al (2014) A multinuclear 1H, 13C and 11B solid-state MAS NMR study of 16- and 18-electron organometallic ruthenium and osmium carborane complexes. Dalton Transactions. 43: 4945-4949.
    Link to publisher’s version
    http://dx.doi.org/10.1039/C3DT53589D
    Type
    Article
    Collections
    Life Sciences Publications

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