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Selective synthesis of Neu5Ac2en and its oxazoline derivative using BF3.Et2O

Ribeiro Morais, Goreti
; 
Oliveira, Rudi S.
; 
Falconer, Robert A.
Publication Date
2009-01-22
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Keywords
Neu5Ac2en, Lewis acid, Sialic acid, Glycal, Oxazoline, REF 2014
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Abstract
Application of the Lewis acid BF3·Et2O to the selective synthesis of 5-acetamido-2,6-anhydro-3,5-dideoxy-d-glycero-d-galacto-non-2-enonic acid (Neu5Ac2en) and the related oxazoline, methyl 7,8,9-tri-O-acetyl-2,3,4,5-tetradeoxy-2,3-didehydro-2,3-trideoxy-4',5'-dihydro-2'-methyloxazolo[5,4-d]- d-glycero-d-talo-non-2-enonate is described.
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http://hdl.handle.net/10454/4616
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Citation
Ribeiro Morais G, Oliveira RS and Falconer RA (2009) Selective synthesis of Neu5Ac2en and its oxazoline derivative using BF3.Et2O. Tetrahedron Letters. 50(14): 1642-1644.
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https://doi.org/10.1016/j.tetlet.2009.01.117
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