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Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion

Crawford, Deborah E.
; 
Wright, L.A.
; 
James, S.L.
; 
Abbott, A.P.
Publication Date
2016-02
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Supervisor
Keywords
Mechanochemical synthesis, Deep Eutectic Solvents (DESs), Twin Screw Extrusion (TSE), Space Time Yields (STYs)
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Peer-Reviewed
Yes
Open Access status
closedAccess
Accepted for publication
2016-02-16
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Life Sciences Publications
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Abstract
Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods
URI
http://hdl.handle.net/10454/17695
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Citation
Crawford DE, Wright LA, James SL et al (2016) Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion. Chemical Communications. 52(22): 4215-4218.
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Link to Version of Record
https://doi.org/10.1039/C5CC09685E
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Article
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