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Identification of an acetyl disulfide derivative in the synthesis of thiosialosides

Ribeiro Morais, Goreti
; 
Oliveira, InĂªs P.F.
; 
Humphrey, Andrew J.
; 
Falconer, Robert A.
Publication Date
2009
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Keywords
Disulfide, Thiosialosides, Chromatography, Magnetic Resonance Spectroscopy
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Abstract
The first report of the formation of an acetyl disulfide sialoside during the synthesis of thioglycosides is described. This compound is a by-product in the synthesis of the 2-thioacetyl sialoside commonly used in thioglycoside preparation. Our investigations into the identification of this novel disulfide are described.
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http://hdl.handle.net/10454/4614
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Citation
Ribero Morais, G., Oliveira, I.P.F., Humphrey, A.J. and Falconer, R.A. (2009). The first report of the formation of an acetyl disulfide sialoside during the synthesis of thioglycosides is described. This compound is a by-product in the synthesis of the 2-thioacetyl sialoside commonly used in thioglycoside preparation. Our investigations into the identification of this novel disulfide are described.. Carbohydrate Research. Vol. 345, No. 1, pp. 160-162.
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https://doi.org/10.1016/j.carres.2009.10.017
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